FIELD: chemistry.
SUBSTANCE: initial raw material in the form of a briquette of a powder of aluminium-magnesium spinel with stoichiometric composition, alloyed with 1 wt % of lithium fluoride is sintered in vacuum at a temperature of 1100-1500°C. The obtained briquette with a diameter equal to the diameter of the mould is loaded into the mould, with its further compression at a temperature of 1550-1600°C for 5-30 minutes under pressure of 350-500 kg/cm2, kept for 30-55 minutes and cooled.
EFFECT: obtaining a polycrystalline optical material from aluminium-magnesium spinel.
1 ex, 1 tbl
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Authors
Dates
2014-07-20—Published
2013-02-21—Filed