FIELD: chemistry.
SUBSTANCE: invention relates to the chemical and oil-processing industry. The invention deals with a method of obtaining an oil plasticiser, which includes purification of oil fractions with selective solvents. An extract is preliminarily diluted with a ketone-aromatic solvent or the ketone-aromatic solvent with a mixture with n-methylpyrrolidone or dimethylsulphoxide with a weight ratio extract:solvent of 1:0.1-0.5. Extraction is carried out at a temperature of 25-55°C by the ketone-aromatic solvent or a mixture of polar solvents: acetone, which contains 5-30% of n-methylpyrrolidone or dimethylsulphoxide with a weight ratio extract:mixture of polar solvents of 1:3.5-4.0 in the presence of an anti-solvent, reducing the diluting ability and increasing the selectivity of the solvent, and as such applied is a water solution of 10-25% concentration of sodium hydroxide or iron sulphate in a quantity of 10-50% to a raw material, obtained raffinate is applied as the target product.
EFFECT: obtaining an ecologically safe plasticiser with low content of polycyclic arenes (PCA) and general sulphur.
2 cl, 1 tbl, 7 ex
Title | Year | Author | Number |
---|---|---|---|
METHOD OF PRODUCING BASE OIL HAVING LOW CONTENT OF SULPHUR AND ECOLOGICALLY CLEAN AROMATIC FILLER MATERIALS AND CAOUTCHOUC AND RUBBER PLASTICISERS | 2010 |
|
RU2450045C1 |
PETROLEUM FEEDSTOCK SEPARATION PROCESS | 2002 |
|
RU2235116C1 |
LUBE FRACTION PURIFICATION PROCESS | 2004 |
|
RU2297440C2 |
LUBE FRACTION PURIFICATION PROCESS | 2003 |
|
RU2243986C1 |
OIL FRACTION PURIFICATION METHOD | 2009 |
|
RU2400526C1 |
METHOD FOR DEPARAFFINATION OF PARAFFINACEOUS OIL FRACTIONS | 2002 |
|
RU2214443C1 |
METHOD OF PRODUCING NON-CARCINOGENIC AROMATIC PROCESS OIL | 2012 |
|
RU2581649C2 |
METHOD FOR PRODUCING NON-CARCINOGENIC AROMATIC PROCESS OIL | 2014 |
|
RU2550823C1 |
METHOD OF OBTAINING PROTECTIVE WAX | 2004 |
|
RU2343186C2 |
PLASTICIZER PREPARATION METHOD AND PLASTICIZER | 2006 |
|
RU2313562C1 |
Authors
Dates
2014-10-20—Published
2012-12-25—Filed