FIELD: chemistry.
SUBSTANCE: method includes oxidative hydrolysis of aqueous solutions of iron sulphate (II) at a temperature of 15 to 40°C and pH of the reaction medium of 4 to 12 followed by hydrothermal treatment of the resulting suspension of iron oxyhydroxides (III) at a temperature of 160 to 230°C. And before the oxidative hydrolysis stage begins, additives are added to the reaction medium, which stabilise the crystal growth. Such additives are polyphosphates or sodium silicates in an amount of 1 to 50 mmoll per 1 mole of iron oxyhydroxide (III).
EFFECT: improvement of qualitative indicators of the red iron oxide pigment due to reduction of its polydispersity in 1,25-1,4 times in comparison with the nearest analogue.
1 tbl, 3 ex
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Authors
Dates
2018-01-09—Published
2016-10-28—Filed