FIELD: chemical or physical processes.
SUBSTANCE: invention relates to a method of producing lignin-melamine-phenol-formaldehyde resin. Disclosed is a method of producing lignin-melamine-phenol-formaldehyde resin, which is carried out by mixing phenol, formaldehyde and a lignin-containing substance in an alkaline medium, wherein melamine is additionally used, and lignin-containing substance used is sodium lignosulphonate; formalin and sodium lignosulphonate are dosed into the reactor, then the reaction mixture is heated to 70–90 °C and held for 1–3 hours, then the content is cooled to 30–50 °C, then alkali and phenol are dosed and heated to 70–90 °C, then holding the reactor contents for 1–6 hours, after holding the reaction mixture is cooled to 40–65 °C and melamine is dosed, the mixture is heated to 70–80 °C and held for 1–4 hours; wherein phenol, formalin and alkali are dosed in molar ratio as 1:(1.5–3):(0.02–0.2), respectively, sodium lignosulphonate and melamine are also prepared in amount of 0.1 to 35% and 0.1 to 20% of the total weight of the prepared phenol, formalin and alkali.
EFFECT: obtaining lignin-melamine-phenol-formaldehyde resin, which provides high strength and water resistance of the adhesive joint.
1 cl, 1 tbl, 3 ex
Title | Year | Author | Number |
---|---|---|---|
METHOD OF PRODUCING LIGNIN-PHENOL-FORMALDEHYDE RESIN | 2023 |
|
RU2820520C1 |
METHOD FOR PRODUCING LIGNOPHENOL-FORMALDEHYDE RESIN | 2023 |
|
RU2812555C1 |
METHOD FOR PRODUCTION OF MODIFIED PHENOL-FORMALDEHYDE RESIN | 1995 |
|
RU2100381C1 |
METHOD OF PREPARING CARBAMIDOFORMALDEHYDE RESINS | 1996 |
|
RU2121482C1 |
BINDER FOR LOW-TOXIC WOOD PLASTIC MATERIALS | 1999 |
|
RU2162860C2 |
METHOD OF MANUFACTURING PHENOL-FORMALDEHYDE OLIGOMER | 2013 |
|
RU2534544C1 |
METHOD OF MODIFIED PHENOLFORMALDEHYDE RESIN PRODUCTION | 0 |
|
SU1786042A1 |
METHOD OF PRODUCING LIGNO-PHENOL-FORMALDEHYDE RESIN | 2009 |
|
RU2423390C2 |
METHOD OF SYNTHESIS OF CARBAMIDOFORMALDEHYDE OLIGOMERIC ADDITIVE TO CARBAMIDE RESINS | 1992 |
|
RU2050372C1 |
PROCESS FOR PREPARING MODIFIED AMINOFORMALDEHYDE RESINS | 1990 |
|
RU2026309C1 |
Authors
Dates
2024-06-04—Published
2023-03-23—Filed