PROCESS FOR PREPARING 2,4-DICHLORONITROBENZOYLACETIC ACID ETHYL ESTER Russian patent published in 1997 - IPC

Abstract SU 1340058 A1

FIELD: synthesis of biologically active compounds. SUBSTANCE: new compound is prepared by new process. Acetic acid ester is prepared from 2,4- dichloro-5-nitrobenzoylacetic acid chloride and ethoxymagnesium malonic ester in the presence of inert organic solvent. The resulting product is subjected to hydrolysis with saturated sodium chloride solution during boiling. Claimed process makes it possible to obtain 81% acetic acid ethyl ester and widen range of raw materials for synthesizing compounds having useful properties. EFFECT: more efficient preparation process.

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SU 1 340 058 A1

Authors

Glushkov R.G.

Levshin I.B.

Marchenko N.B.

Zajtseva A.V.

Dates

1997-03-27Published

1985-12-17Filed