FIELD: organic chemistry, chemical technology. SUBSTANCE: product: 1,2-bis-(1-glycidylbenzimidazole-2-ylthio)-ethane, empirical formula is C22H2N4O4S2, yield is 87%, m. p. is 158-162 C; 1,2-bis-(benzimidazole-2-ylthio)-ethane, empirical formula is C16H14N4S2, yield is 60%, m. p. is 264-266 C. Reagent 1: benzimidazolethione-2. Reagent 2: dibromoethane. Reaction conditions: alkaline spirituous medium. Reagent 3: 1,2-bis-(benzimidazole-2-ylthio)-ethane. Reagent 4: epichlorohydrin. Reaction condition: in the presence of alkali. EFFECT: improved method of synthesis, increased yields. 7 ex, 1 tbl
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Authors
Dates
1998-02-20—Published
1990-09-04—Filed