1,2-BIS-(1-GLYCIDYLBENZIMIDAZOLE-2-YLTHIO)-ETHANE AS COHARDENING AGENT OF EPOXY RESINS AND 1,2-BIS-(BENZIMIDAZOLE-2-YLTHIO)-ETHANE AS AN INTERMEDIATE COMPOUND FOR SYNTHESIS OF 1,2-BIS-(1-GLYCIDYLBENZIMIDAZOLE-2-YLTHIO)-ETHANE AS COHARDENING AGENT OF EPOXY RESINS Russian patent published in 1998 - IPC

Abstract SU 1743160 A1

FIELD: organic chemistry, chemical technology. SUBSTANCE: product: 1,2-bis-(1-glycidylbenzimidazole-2-ylthio)-ethane, empirical formula is C22H2N4O4S2, yield is 87%, m. p. is 158-162 C; 1,2-bis-(benzimidazole-2-ylthio)-ethane, empirical formula is C16H14N4S2, yield is 60%, m. p. is 264-266 C. Reagent 1: benzimidazolethione-2. Reagent 2: dibromoethane. Reaction conditions: alkaline spirituous medium. Reagent 3: 1,2-bis-(benzimidazole-2-ylthio)-ethane. Reagent 4: epichlorohydrin. Reaction condition: in the presence of alkali. EFFECT: improved method of synthesis, increased yields. 7 ex, 1 tbl

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SU 1 743 160 A1

Authors

Korotkikh N.I.

Kozlov A.V.

Shvajka O.P.

Kochergin Ju.S.

Kulik T.A.

Dates

1998-02-20Published

1990-09-04Filed