FIELD: organic chemistry. SUBSTANCE: product: 1,3-bis-(2,3-epithiopropyl)-benzimidazolone-2 of the formula: . Empirical formula is C13H10N2OS2, yield is 69%, m. p. is 116-118 C. Reagent 1: 1-(2,3-epithiopropyl)-3-(2,3-epoxypropyl)-benzimidazolone-2. Reagent 2: thiourea. Reaction conditions: in methanol medium, at room temperature. EFFECT: improved method of synthesis, increased yield. 1 ex, 1 tbl
Title | Year | Author | Number |
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1-(2,3-EPOXYPROPYL)-3-(2,3-EPITHIOPROPYL)-BENZIMIDAZOLONE-2 AS MONOMER FOR HEAT-PROOF GLUE COMPOSITIONS | 0 |
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EPOXY GLUE COMPOSITION | 1992 |
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GLUE COMPOSITION | 1992 |
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METHOD OF OBTAINING 1-(2,3-EPYTHIOPROPYL)-3-(2,3-EPOXYPROPYL)-BENZIMIDAZOLON-2 | 0 |
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Authors
Dates
1998-02-20—Published
1990-09-04—Filed