FIELD: organic chemistry. SUBSTANCE: product: 2-methyl-4-(benzimidazolyl-2')-quinoline dimethylsulfate binary salt dihydrate (IK-150), empirical formula is C26H32N6SO4•2H2O., yield is 62%, m. p. is 222-223 C. Product: 2-phenyl-4-(benzimidazolyl- -2')-quinoline diethylsulfate binary salt (IK-120), empirical formula is C48H42N6SO5,, yield is 56%, m. p. is 274 C. Reagent 1: substituted derivatives of 4-(benzimidazolyl-2')-quinoline. Reagent 2: dialkyl sulfate. Conditions: heating in medium of organic solvents. EFFECT: improved method of synthesis, increased yield. 3 tbl, 2 ex
Authors
Dates
1998-04-10—Published
1990-07-09—Filed