FIELD: organic chemistry. SUBSTANCE: product: trans-2-N,N-dimethylaminopinocamphone oxime, empirical formula is C12H22N20, yield is 67%, m. p. is 114.5-116 C; its hydrochloride, empirical formula is C12H23N2OCl, m. p. = 220 C (with sublimation). Reagent 1: α-pinene. Reagent 2: isoamylnitrite and hydrochloric acid. Reaction conditions: alcohol, acetic acid. Prepared a-pinene nitrosochloride is treated with aqueous solution of dimethylamine. Synthesized compounds were used in agriculture as insecticides. EFFECT: improved method of synthesis. 5 tbl
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Authors
Dates
1995-03-20—Published
1990-06-26—Filed