PROCESS FOR RECOVERING BENAZOLE P FROM BOTTOM RESIDUES OF ITS PRODUCTION Russian patent published in 1994 - IPC

Abstract RU 2008310 C1

FIELD: organic chemistry. SUBSTANCE: bottom residues is treated with aqueous solution of sodium hydroxide in mixing ratio of 3-4 % by weight in presence of ethylene glycol at temperature of 101-105 C, with weight ratio of melted bottom residue, sodium hydroxide and ethylene glycol being 1: (3.3-4.5): (0.8-0.12). The end product is separated at pH ranging from 11.0 to 11.3, yield: 20-26% , m. p. 130 C. EFFECT: increased purity.

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RU 2 008 310 C1

Authors

Litvin B.L.

Mosijchuk A.I.

Mishchenko E.E.

Lavrinenko S.A.

Vasilishin E.V.

Deev A.S.

Sokolyk V.M.

Dates

1994-02-28Published

1991-05-20Filed