FIELD: metalloorganic chemistry. SUBSTANCE: product - trimethylgermyl-(2-trimethylgermyloxy-2-phenyl)-acetate, C14H24O3Ge2, value nD20 = 1.5087. Reagent 1: dimethylaminotrimethylgermanium. Reagent 2: mandelic acid trimethylgermylcarboxylate. Reaction conditions; in the medium of diethyl ether or methylene chloride at heating for 30 min. EFFECT: improved method of synthesis.
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Authors
Dates
1994-10-15—Published
1991-05-30—Filed