FIELD: organic chemistry. SUBSTANCE: product: P3N3Cl6-4(OAr)u, where n= 1-6, Ar - n-NO2C6H4i;2,4-C6H3(NO3)2i, gross-formulas are: C36H24N9P3O18, C30H20ClN8O15, C24H16Cl2N7P3O12, C18H12Cl3N6P3O9, C6H4Cl5N4P3O3, C36H18N15P3O30. Yield is 85-95%. Reagent 1: HO-Ar, where Ar - as indicated above. Reagent 2: P3N3Cl6. Reaction conditions: in the presence of , where X - halide, Y - , , , , , in two-phase system, organic solvent-water, alkali, at pH 11-12, at 20-30 C. EFFECT: enhanced yield of products. 3 tbl
Title | Year | Author | Number |
---|---|---|---|
ISOTHIURONIUM AZINES SHOWING ANTITUMORAL ACTIVITY | 1991 |
|
RU2032676C1 |
1,3-BIS-(2,3-DIACRYLOYL OXYPROPYL)-5,5-DIMETHYL-2,4-IMIDAZOLIDINE DION AS MODIFIER FOR PHOTOPOLYMERIZED ACRYLATE COMPOSITIONS | 1991 |
|
RU2032672C1 |
7-ALKOXY -4-OXA -1,2,6- TRINITRATEHEPTANETRIOLS SHOWING CARDIOTONIC ACTIVITY | 1991 |
|
RU2027700C1 |
METHOD OF PRODUCING ARENSELENONIC ACIDS | 0 |
|
SU1293176A1 |
N,N-BIS-(4-HYDROXYPHENOXY)-FLUORINE-SUBSTITUTED ARYLS AS MONOMERS FOR THERMOSTABLEPOLYMERS | 0 |
|
SU1048679A1 |
1,2-BIS-(1-GLYCIDYLBENZIMIDAZOLE-2-YLTHIO)-ETHANE AS COHARDENING AGENT OF EPOXY RESINS AND 1,2-BIS-(BENZIMIDAZOLE-2-YLTHIO)-ETHANE AS AN INTERMEDIATE COMPOUND FOR SYNTHESIS OF 1,2-BIS-(1-GLYCIDYLBENZIMIDAZOLE-2-YLTHIO)-ETHANE AS COHARDENING AGENT OF EPOXY RESINS | 1990 |
|
SU1743160A1 |
PROCESS FOR PURIFYING PHENOLIC WASTE WATER | 0 |
|
SU1745694A1 |
METHOD OF PRODUCING 4-(METHYLAMINO)-BIPHENYL | 0 |
|
SU1512966A1 |
COMPOSITION OF FILM COATING FOR TEMPORARY ANTICORROSION PROTECTION | 1990 |
|
RU2034885C1 |
1-GLYCIDYL-2-METALLYLTHIO-4,5-DIPHENYLIMIDAZOLE AS COHARDENING AGENT OF EPOXY RESINS | 1990 |
|
SU1743169A1 |
Authors
Dates
1994-10-15—Published
1990-07-30—Filed