FIELD: organic chemistry. SUBSTANCE: product - monopropylene glycol ester of aliphatic, naphthenic or aromatic acid of formula (I) . Yield is 94.5-96.5% , m. p. is 139-154 C/2 mm mercury column. Reagent 1: aliphatic or naphthenic or aromatic acid. Reagent 2: monopropylene glycol. Reaction conditions: heating at 155-160 C at mole ratio of reagents 1 and 2 = 1: (1.8-2) in the presence of catalyst - natural zeolite-clinoptilolite. Method is used in chemistry of glycol esters. EFFECT: improved method of synthesis. 2 tbl
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Authors
Dates
1994-11-15—Published
1991-11-29—Filed