FIELD: metallurgy. SUBSTANCE: product - higher N-acyl-N1, N2-triphenyl-β-aminoisobutyrylamidinium chlorides of the formula PhN(CnH2n+1C=O)CH2C(CH3)H-C-NHPh[(+)NHPh)Cl- where n = 8, 10, 17, empirical formula is C31H40ClN30, m. p. is 159-160 C, yield is 92%. Empirical formula is C33H44ClN30, m. p. is 166-168 C, yield is 95%. Empirical formula is C40H58ClN30, m. p. is 148-150 C, yield is 89%. Reagent 1: acylchlorides. Reagent 2: N, N1, N2-triphenyl-β-aminoisobutyrylamidine. Reaction conditions: anhydrous ethyl ether. EFFECT: improved method of synthesis. 2 tbl
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Authors
Dates
1994-12-15—Published
1992-03-17—Filed