FIELD: organic chemistry. SUBSTANCE: product of the formula , empirical formula is C2H7TiP2O8,5, yield is 60 g (97.3% ), m. p. is 300 C, molecular mass is 277. Reagent 1: tetrabutoxybutane. Reagent 2: ortho-phosphoric acid. Reaction conditions: ratio of reagent 1 and 2 is 1:2, respectively, in the medium of aromatic hydrocarbon, at 80-90 C. Butanol formed is removed. EFFECT: improved method of synthesis.
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Authors
Dates
1995-05-20—Published
1991-04-24—Filed