FIELD: organic chemistry. SUBSTANCE: to utilize strong poisoning substance - mustard gas the latter is interacted with acetylene at 400-700 C (preferably at 550-660 C), at molar ratio of reagents 1:(1-3) following by rectification. Thiopene yield is 45-50%, mustard gas conversion is 100%. Method is used for synthesis of medicinal agents. EFFECT: improved method of synthesis. 2 cl
Title | Year | Author | Number |
---|---|---|---|
METHOD OF PRODUCING THIOPHEN AND THIENOTHIOPHENONS | 0 |
|
SU1442522A1 |
0 |
|
SU1776655A1 | |
METHOD OF OBTAINING THIOLES | 0 |
|
SU930878A1 |
PROCESS FOR PREPARING BIS-2-CHLOROETHYLSULFOXIDE | 1993 |
|
RU2034833C1 |
PROCESS OF UTILIZATION OF YPERITE | 1993 |
|
RU2039039C1 |
METHOD OF PRODUCING BENZ(B)THIOPHENE OR ITS DERIVATIVES | 0 |
|
SU1583420A1 |
PROCESS FOR PRODUCING THIOPHENE | 0 |
|
SU910634A1 |
METHOD FOR PRODUCTION OF CIS-1,2-DI(ALKYL SELENO) ETHENES | 1991 |
|
SU1833615A3 |
CATALYTIC PROCESS FOR PREPARING THIOPHENE AND 2-THIOPHENE-THIOL | 2014 |
|
RU2564675C1 |
METHOD OF UTILIZATION OF YPRITE | 1998 |
|
RU2139856C1 |
Authors
Dates
1995-06-09—Published
1992-12-21—Filed