1,3-BIS-[DIMETHYL(TERT-BUTYLAMINO)SILYL]-2,2,4,4-TETRAMETHYLC- YCLODISILAZANE AS AN INITIATING AGENT OF GROWTH AND MULTIPLICATION OF HETEROTROPHIC BACTERIA, AND A METHOD OF ITS SYNTHESIS Russian patent published in 1995 - IPC

Abstract RU 2036927 C1

FIELD: organic chemistry. SUBSTANCE: product: 1,3-bis-[dimethyl(tert. -butylamino)silyl] -2,2,4,4-tetramethyl- cyclodisilazane, empirical formula is C16H44N4SiH, yield is 95%, И2д

0 = 1.4525, b. p. is 102-104 C/2 mm mercury column. Reagent 1: 1,3-bis-(dimethylchlorosilyl)-2,2,4,4-tetramethylcyclodisilaz- ane. Reagent 2: tert.-H2NC4-H9. Reaction conditions: in mixture of toluene and butylacetate, at 15-35 C. EFFECT: improved method of synthesis. 3 cl, 3 tbl

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RU 2 036 927 C1

Authors

Varezhkin Ju.M.

Mikhajlova A.N.

Kosareva M.S.

Klement'Ev I.Ju.

Stetsik N.Ja.

Novikov V.I.

Simakov Ju.G.

Ermakova V.Ja.

Dates

1995-06-09Published

1990-10-31Filed