FIELD: organic chemistry. SUBSTANCE: method involves acetoxylation of trioxane with acetic anhydride at the molar ratio trioxane/anhydride 1: (1.1-1.3), at 100-120 C using sulfocationic exchanger in acid form as a catalyst. Method is used for methylenediacetate synthesis. EFFECT: improved method of synthesis.
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Authors
Dates
1995-07-20—Published
1993-02-15—Filed