FIELD: chemistry; methods for assaying organic compounds. SUBSTANCE: this method for manufacturing sorbent designed for gas-liquid chromatographic analysis of thermolabial organic compounds using apiesones as stationary liquid phase includes such steps as application of liquid phase to solid carrier, thermal conditioning of resultant sorbent, suppressing activity of stationary liquid phase causing thermal disintegration of organic compounds in packed column with ammonia, standing dry sorbent after application of liquid phase at temperature of about 420 to 490 C in ammonia-containing atmosphere at partial pressure of about 0.005 to 0.6 MPa during 2 to 8 h. EFFECT: irreversible suppression of catalytic activity of stationary phase. 5 cl, 2 dwg
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Authors
Dates
1995-07-20—Published
1992-11-23—Filed