FIELD: chemical technology. SUBSTANCE: product: formylbutyric acid methyl ester, empirical formula is C5H8O3, b. p. is 82-84 C at 7 mm mercury column. Reagent 1: glutaraldehyde. Reagent 2: hydrogen peroxide. Reaction conditions: in methanol medium, in the presence of acid catalyst, at mole ratio aldehyde peroxide 1:(0.4-10), respectively. Before boiling prepared mass is kept at the room temperature for 12 h. EFFECT: improved method of synthesis. 1 tbl
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Authors
Dates
1995-08-27—Published
1992-09-18—Filed