FIELD: chemical industry. SUBSTANCE: the product: thioglycolic acid salts. Reagent 1: as a source of monochloroacetic acid a preneutralized monochloroacetic acid waste product resulting from recovery of monochloroacetic acid, or a reaction mixture after chlorination of acetic acid. Reagent 2: thiourea. Reaction conditions: the ratio is 1:1-1.1. Reagent 3: intermediate 5-formamidinothioacetic acid. Reagent 4: the base is monoethanolamine or alkali. Reagent 5: acid. EFFECT: more efficient preparation process. 1 tbl
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Authors
Dates
1995-09-27—Published
1992-03-09—Filed