FIELD: organic synthesis. SUBSTANCE: desired product is prepared by alkylation of alkyl phenol with lower aliphatic secondary alcohol. The process is carried out at elevated temperature with the help of catalyst. Phosphorous-tungsten heteropolyacid having formula H7PW12042 is used as said catalyst. P-cresol is used as aforementioned origin phenol, methyl-tert-butyl carbinol is used as alkylating agent. Alkylation is carried out at 85-120 C, molar ratio of p-cresol and alcohol being 1.9-1. Quantity of catalyst is 1-2 % of mass of p-cresol. EFFECT: improves efficiency of the method. 2 cl
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Authors
Dates
1996-08-20—Published
1994-04-07—Filed