FIELD: organic chemistry. SUBSTANCE: method involves adding amine solution into phosgene solution followed by heating reaction mixture and by isolation of desired product. Mentioned above adding is carried out by elimination of heat within 60-280 s, initial temperature being (-3)-(-9) C, final temperature being 15-25 C. EFFECT: improves efficiency of method. 1 tbl
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Authors
Dates
1995-12-10—Published
1991-05-05—Filed