FIELD: organic chemistry. SUBSTANCE: phthalonitrile is used as reagent 1, sodium butylate is used as reagent 2, phenyl diamine is used as reagent 3, urea being used as reagent 4. reaction is carried out by boiling reaction mixture within 5-6 h. Yield of desired triisoindole benzene macrocycle is 95.5 %, its melting point being 331-332 C. EFFECT: improves efficiency of method. 2 dwg, 2 tbl
Authors
Dates
1996-02-20—Published
1994-03-16—Filed