FIELD: organic chemistry. SUBSTANCE: tetraazaporphyne magnesium complex (MgTAP) is synthesized by interaction of maleic acid dinitrile with magnesium alcoholate in medium of an organic solvent where magnesium 1-butylate is used as magnesium alcoholate and 1-butanol is used as an organic solvent. Process is carried out at slow heating the reaction mass from 25 to 90 C for 50-70 min. MgTAP can be used as a semiproduct for synthesis of catalysts of redox and polymerization reactions in dye and semiconductor production. Method ensures to decrease process time, eliminates the stage of preliminary solvent drying. EFFECT: increased yield, improved method of synthesis. 1 dwg, 2 tbl, 5 ex
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Authors
Dates
1999-08-27—Published
1995-04-19—Filed