FIELD: chemical industry. SUBSTANCE: product: 4,4I-polythiobis (2,6-di-tert-butylphenols) of empirical formula: BF C28H4202S(1-9). Yield: 99.5%. Reagent 1: 2,6-di-tert-butylphenol. Reagent 2: sulfur. Reaction conditions: solvent-dimethylformamide or dimethylacetamide, temperature is higher or equal to 130 C, and air or inert gas is fed. EFFECT: more efficient preparation process.
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Authors
Dates
1996-10-27—Published
1994-07-11—Filed