FIELD: chemical technology, polymers. SUBSTANCE: method involves polycondensation of pyromellitic acid dianhydride, 1,12-dodecamethylenediamine or 1,10-decamethylenediamine, or mixture of above indicated diamines at mole ratio from (0.99:0.01) to (0.01:0.99), respectively. Additionally, diphenyloxidetetracarboxylic acid dianhydride is added to reaction medium at mole ratio of pyromellitic acid dianhydride and diphenyloxidetetracarboxylic acid dianhydride from (0.99:0.01) to (0.05:0.95), respectively. Obtained polyimides were processed under pressure by extrusion and casting method. EFFECT: improved method of synthesis. 1 tbl
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Authors
Dates
1996-11-27—Published
1993-02-24—Filed