1-IODO-3,4-DICHLORO-3,4,4-TRIFLUOROBUTYL ACETATE AS INTERMEDIATE PRODUCT FOR PRODUCTION OF 1,1,2-TRIFLUORO-1-BUTENE-4-OL BEING USED IN SYNTHESIS OF POLYFLUORINATED SURFACTANTS FOR COPOLYMERIZATION AND PRODUCTION OF ELECTROLYTES Russian patent published in 1997 - IPC

Abstract RU 2074168 C1

FIELD: production of surfactants, processes of copolymerization. SUBSTANCE: desired compound having formula CF2-CFCl-CH2-CHJ-OCOCH3 is prepared by addition reaction of 1,2-dichloro-1,2,2-trifluoriodoethane and vinyl acetate. The process takes place at 25-40 C within 1-3 h in the presence of initiating mixture in aqueous-acetonitrile solution. Sodium dithionate and sodium bicarbonate are used as said initiating mixture. EFFECT: improves quality of desired product.

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RU 2 074 168 C1

Authors

Gorbunova T.I.

Zapevalov A.Ja.

Saloutin V.I.

Dates

1997-02-27Published

1995-03-21Filed