FIELD: organic chemistry. SUBSTANCE: 1-chloroalkane is used as reagent 1, 1.1-dimethyl hydrazine being used as reagent 2. Reaction is carried out at 75-85 C within 3-5 h, molar ratio of said reagents being 1:1.3-2.0 respectively. Yield of desired product is 82-92 %. EFFECT: improves efficiency of the method. 2 tbl
Title | Year | Author | Number |
---|---|---|---|
METHOD OF PREPARING GLYCIN-2D | 2000 |
|
RU2170725C1 |
METHOD OF RENDERING HARMLESS OF FLUOROCHLOROHYDRACARBONS | 1995 |
|
RU2091107C1 |
METHOD OF DETERMINING UNSYMMETRICAL DIMETHYLHYDRAZINE IN SOILS AND VEGETABLE MATERIALS | 1985 |
|
RU2122198C1 |
PROCESS FOR PREPARING ETHANOL HALIDE | 1992 |
|
RU2039034C1 |
METHOD OF DISINTOXICATION OF METALLIC SURFACES POLLUTED BY HYDRAZINE- BASED COMPONENTS OF ROCKET FUEL | 1996 |
|
RU2101390C1 |
METHOD OF PREPARING 1-FLUOR-1,1-DICHLOROETHANE, 1,1-DIFLUORO 1-CHLOROETHANE, 1,1,1-TRIFLUOROETHANE AND REACTION UNIT DEVICE FOR CARRYING IT THROUGH | 1998 |
|
RU2160245C2 |
METHOD OF PREPARING CARBON-14 MARKED CARBON DIOXIDE | 1997 |
|
RU2121966C1 |
METHOD OF PHOTOCOLORIMETRIC DETECTION OF ASYMMETRICAL DIMETHYLHYDRAZINE IN AQUEOUS SOLUTIONS | 1981 |
|
RU2114417C1 |
METHOD OF PREPARING N-ACETYLPHENYLALANINE | 1995 |
|
RU2087464C1 |
METHOD OF DETERMINING UNSYMMETRICAL DIMETHYLHYDRAZINE | 1987 |
|
RU2111486C1 |
Authors
Dates
1997-02-27—Published
1992-06-18—Filed