FIELD: chemical industry. SUBSTANCE: product: 2-alkyl-5,6,7,8-tetrahydro-9,10-anthaquinone. Reagent 1: anthracene. Reagent 2: hydrogen. Reaction conditions: in the presence of nickel or palladium catalyst followed by alkylation of the resulting mixture with olefin or halogen alkyl in the presence of aluminium chloride or alumosilicate catalyst followed by oxidation in acetic acid in the presence of hydrogen peroxide and chromic anhydride. EFFECT: more efficient preparation process. 2 dwg, 6 tbl
Title | Year | Author | Number |
---|---|---|---|
METHOD OF PREPARATION OF SKELETON CATALYST FOR SELECTIVE HYDROGENATION OF ANTHRAQUINONES | 0 |
|
SU1754155A1 |
METHOD FOR PREPARING 4,4-DIMETHYL-1-(PARA-CHLOROPHENYL)-PENTANE-3-ONE | 2002 |
|
RU2228327C1 |
PROCESS FOR PRODUCING 1,2,3,4-TETRAHYDROANTHRACENEDIOL-9,10 (MODIFICATIONS) | 0 |
|
SU965348A3 |
0 |
|
SU549077A3 | |
METHOD OF PRODUCING HYDROGEN PEROXIDE | 2018 |
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RU2687449C1 |
0 |
|
SU502602A3 | |
0 |
|
SU510145A3 | |
PROCESS FOR PREPARING DERIVATIVES OF IMIDAZO(1,2-A)PURINE OR THEIR ACID ADDITION SALTS | 0 |
|
SU1066463A3 |
METHOD FOR PREPARING SEROTONIN AND ITS PHARMACOLOGICAL SALTS | 2002 |
|
RU2227140C1 |
METHOD FOR PRODUCTION OF 9,10-BIS(PHENYL ETHYNYL)ANTHRACENE AND ITS DERIVATIVES | 1992 |
|
RU2054406C1 |
Authors
Dates
1997-05-27—Published
1992-05-07—Filed