FIELD: tire and rubber industries. SUBSTANCE: e-caprolactam- blocked toluilenediisocyanate (mixture of 2,4- and 2,6-isomers in ratio 80:20 to 65: 35) is granulated by sprinkling melt of product with melting temperature 140-150 C and 1-2 wt.-% of free e- caprolactam into water with temperature not higher than 30 C followed by filtration and drying of granules with air at 30-35 C. EFFECT: optimized parameters of process.
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RU2107709C1 |
Authors
Dates
1997-06-10—Published
1995-03-01—Filed