METHOD OF PHOTOMETRIC DETERMINATION OF 1-METHYL-1,2-DICYCLOPROPYLCYCLOPROPANE IN SOILS AND VEGETAL MATERIALS Russian patent published in 1997 - IPC

Abstract RU 2086960 C1

FIELD: analytical chemistry; testing for contamination of soils with toxicant - 1-methyl-1,2-dicyclopropylcyclopro- pane. SUBSTANCE: method includes treatment of analyzed sample with ethyl alcohol or water-alcohol mixture with mass ratio of 1: (2.0-3.0). Obtained mixture is thoroughly agitated and held still for 15-20 min. Then, mixture is heated up to 98-100 C with air bubbling at rate of 0.1-0.2 l/min through successively installed vessels with analyzed sample and concentrated sulfuric acid. Added to concentrated sulfuric acid is solution of para-dimethylaminobenzaldehyde in aqueous solution of hydrochloric acid and ethyl alcohol. Optical density of colored solution is measured and its value serves to find the content of 1-methyl-1,2- dicyclopropylcyclopropane in soil. EFFECT: higher efficiency. 2 tbl

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RU 2 086 960 C1

Authors

Potrokhov V.K.

Timofeeva A.M.

Dates

1997-08-10Published

1993-07-02Filed