METHOD OF PREPARING PURIFIED TEREPHTHALIC ACID (VARIANTS) Russian patent published in 1997 - IPC

Abstract RU 2094424 C1

FIELD: chemical industry. SUBSTANCE: claimed method for preparing terephthalic acid comprises catalytically oxidizing para-xylene in liquid phase to obtain raw terephthalic acid containing 4-carboxy benzaldehyde as the main impurity, and treating raw terephthalic acid with hydrogen in the presence of hydrogenation catalyst in reaction vessel to obtain purified terephthalic acid containing 4-carboxy benzaldehyde in fixed amount which makes it possible to achieve stationary state after partially deactivated catalyst is replaced by new catalyst. The claimed method comprises feeding into reactor raw terephthalic acid which contains 4-carboxy benzaldehyde in amount that exceeds amount in stationary state, and treating terephthalic acid till said treatment attains stationary state. EFFECT: more efficient preparation method. 6 cl, 1 tbl

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RU 2 094 424 C1

Authors

Norio Taniguti[Jp]

Khirosi Jamane[Jp]

Dates

1997-10-27Published

1991-07-03Filed