METHOD OF SYNTHESIS OF DICHLORO-DI-PARA-XYLYLENE Russian patent published in 1998 - IPC

Abstract RU 2101272 C1

FIELD: organic chemistry. SUBSTANCE: method involves photochemical chlorination of 2-chloro-p-xylene at 160-170 C, interaction of 2-chloro-p-xylyl chloride with trimethylamine at 0-5 C, thermic cleavage of 2-chloro-p-methylbenzyltrimethylammonium chloride in concentrated alkali solution at 110-120 C. The synthesized semiproduct is used for synthesis of poly-p-xylylenes used in electronics. EFFECT: increased yield, simplified technology of process.

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RU 2 101 272 C1

Authors

Belova T.P.

Pavljuk N.F.

Khorkin A.A.

Volod'Ko Ju.A.

Pashkov M.A.

Savitskij A.M.

Dates

1998-01-10Published

1996-08-01Filed