FIELD: analytical methods. SUBSTANCE: invention aims at increasing rapidity in determining leakage in process equipment. Chemical oxygen minimum in circulating water is determined via oxidation by aqueous solution of potassium bichromate, silver sulfate, mercury sulfate, sulfuric acid, and phosphoric acid under boiling. Optimal volume ratio of sulfuric acid, phosphoric acid, and water in oxidative solution is 1.5:1:3, optimum boiling time 20 min. EFFECT: reduced analysis time. 2 tbl
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Authors
Dates
1998-12-20—Published
1997-06-30—Filed