METHOD OF SYNTHESIS OF META-HALOIDPHENOLS Russian patent published in 2002 - IPC

Abstract RU 2177932 C1

FIELD: organic chemistry, chemical technology. SUBSTANCE: invention relates to synthesis of m-haloidphenols of the general formula: where X is Br, Cl used in production of dyes, medicinal agents, phenolformaldehyde resins. Method is performed by diazotization of m-aminophenol as meta-derivative of aniline with sodium nitrite. Diazotization is carried out in mixture of hydrohalic acid and acetone. Acetone is taken in the amount 500-1000 vol. p. per 1 mole of m-aminophenol. Obtained diazonium salt is decomposed in the presence of monovalent copper halide at 30-35 C. EFFECT: development of new industrial method of production of m-haloidphenol, broadened raw base. 2 cl

Similar patents RU2177932C1

Title Year Author Number
METHOD OF SYNTHESIS OF 5-AMINOSALICYLIC ACID FOR PHARMACEUTICAL AIMS 1998
  • Bojarintseva O.N.
  • Kabanova I.A.
  • Ivanova L.A.
  • Alekseenko E.M.
RU2155746C2
METHOD OF ISOLATION AND PURIFICATION OF (RR,SS)-2-[(DIMETHYLAMINO)METHYL]-1-(3-METHOXYPHENYL)-CYCLOHEXANOL (TRAMADOL) HYDROCHLORIDE 2001
  • Bychikhina N.N.
  • Knjazeva V.F.
  • Krechetova N.D.
  • Novokshanova L.A.
  • Ostapovich Ju.I.
RU2196765C2
METHOD OF SYNTHESIS OF 2-METHOXY-5-CHLOROBENZOIC ACID 1992
  • Cherdantseva N.M.
  • Nesterov V.M.
  • Gumerova N.V.
RU2030387C1
METHOD OF SYNTHESIS OF BENZHYDROL β-DIMETHYLAMINOETHYL ESTER HYDROCHLORIDE 1992
  • Smetskaja N.I.
  • Rusinova E.V.
  • Sukhorukova R.I.
  • Ljustik A.A.
  • Mukhina N.A.
RU2036899C1
DERIVATIVES OF (1,2,5)-THIADIAZOLO-(3,4-G) INDOLES AND PROCESS FOR PREPARING SAME 0
  • Titov Gennadij Alekseevich
  • Chetverikov Valerij Pavlovich
SU1122659A1
0
  • Gortinskaya Tatyana Vladimirovna
  • Nyrkova Valentina Georgievna
  • Savitskaya Nina Viktorovna
  • Petrova Evgeniya Valentinovna
  • Bondar Larisa Nikolaevna
  • Shchukina Mariya Nikolaevna
  • Klimonova Zoya Mikhajlovna
  • Potapova Varvara Grigorevna
  • Gorodetskij Lev Shlomovich
  • Volzhina Olga Nikolaevna
SU504766A1
METHOD OF SYNTHESIS OF BENZHYDRYL CHLORIDES 2001
  • Morozova N.T.
  • Smetskaja N.I.
  • Kabanova I.A.
RU2196126C1
METHOD OF SYNTHESIS OF 1-ETHYL-2-AMINOMETHYLPYRROLIDINE 1995
  • Semikolenov V.A.
  • Burova O.A.
  • Smirnova N.M.
RU2081111C1
METHOD OF SYNTHESIS OF 1-(PARA-CHLOROBENZHYDRYL)-4-(2-HYDROXYETHYL)-PIPERAZINE 2001
  • Morozova N.T.
  • Smetskaja N.I.
  • Kabanova I.A.
RU2204556C2
METHOD OF PRODUCING ETHYL ESTER OF N-AMINOBENZOIC ACID 0
  • Mogilevskij M.Yu.
  • Sheshina G.I.
  • Ivanova L.A.
SU753069A1

RU 2 177 932 C1

Authors

Knjazeva V.F.

Ostapovich Ju.I.

Mikhajljukova T.L.

Trappel' L.N.

Dates

2002-01-10Published

2000-05-29Filed