METHOD OF SYNTHESIS OF FULLERENES Russian patent published in 2002 - IPC

Abstract RU 2186022 C2

FIELD: chemical technology. SUBSTANCE: evaporation of graphite rods is carried out in reaction zone of working chamber by effect of current discharge with simultaneous effect by energy of electric and electromagnetic fields. The discharge current power is 150-500 A at voltage 26-32 V, electric field intensity is 10-25 A/m2, electromagnetic field intensity is 0.1-0.5 A/m2, induction value is 0.1-1.0 Tl. Method involves the effect acoustic field energy on fullerene-containing mass removing from the reaction zone by three perpendicular reciprocal directions at frequency 25-35 kHz for each and at intensity value 0.5-5.0 dB. This ensures to carry out the ordered and regulated process of removal of fullerene-containing mass with accumulation of fullerene particles. Invention can be used for production of new materials used in different branches of industry. EFFECT: decreased energy consumption, high yield of fullerenes (15-22 wt.-%). 3 cl

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RU 2 186 022 C2

Authors

Burangulov N.I.

Plugin A.I.

Sulima V.V.

Vojtko S.A.

Dates

2002-07-27Published

2000-02-25Filed