FIELD: chemical technology. SUBSTANCE: evaporation of graphite rods is carried out in reaction zone of working chamber by effect of current discharge with simultaneous effect by energy of electric and electromagnetic fields. The discharge current power is 150-500 A at voltage 26-32 V, electric field intensity is 10-25 A/m2, electromagnetic field intensity is 0.1-0.5 A/m2, induction value is 0.1-1.0 Tl. Method involves the effect acoustic field energy on fullerene-containing mass removing from the reaction zone by three perpendicular reciprocal directions at frequency 25-35 kHz for each and at intensity value 0.5-5.0 dB. This ensures to carry out the ordered and regulated process of removal of fullerene-containing mass with accumulation of fullerene particles. Invention can be used for production of new materials used in different branches of industry. EFFECT: decreased energy consumption, high yield of fullerenes (15-22 wt.-%). 3 cl
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Authors
Dates
2002-07-27—Published
2000-02-25—Filed