FIELD: industrial organic synthesis. SUBSTANCE: invention relates to separation of alpha- picoline-water azeotrope mixture formed in solvent regeneration stage in poly- p-phenylene-terephthalamide and consists in that solid sodium hydroxide is added to mixture containing alpha-picoline and water un amounts 0.50-0.66 g per 1 g water, after which resulting suspension is separated. EFFECT: simplified equipment, reduced power consumption, and enabled wasteless production of poly- p-phenylene-terephthalamide. 3 ex
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Authors
Dates
2002-08-27—Published
2001-04-17—Filed