METHOD OF SYNTHESIS OF 2-(2-FURYL)-1,3-DIOXOLANE (FUROLANE) Russian patent published in 2002 - IPC

Abstract RU 2191185 C1

FIELD: organic chemistry of heterocyclic compounds, chemical technology. SUBSTANCE: invention relates to a method of synthesis of 2-(2-furyl)-1,3-dioxolane (furolane) that is used as an intermediate compound in the fine organic synthesis and in agriculture as a substance showing the growth-regulating activity. Method involves the interaction of ethylene glycol with furfurol in the presence of an acidic catalyst and process is carried out under condition of vacuum distillation in the mole ratio ethylene glycol : furfurol : catalyst = 1: (1.33-1.11) : (0.00013-0.0002), respectively, and water formed in a process is removed from the reaction medium by azeotropic distillation with furfurol. EFFECT: decreased amount of catalyst, exclusion of toxic and fire hazard solvent. 1 tbl, 9 ex

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RU 2 191 185 C1

Authors

Vasilin V.K.

Kosulina T.P.

Kul'Nevich V.G.

Nen'Ko N.I.

Parkhomenko A.N.

Smoljakov V.P.

Dates

2002-10-20Published

2001-04-09Filed