FIELD: analytical instrumentation engineering; chromatographic analysis of composition of substances.
SUBSTANCE: proposed method includes delivery of carrier gas to evaporation chamber through gas supply line, introduction of sample into evaporation chamber, delivery of part of gas flow from evaporation chamber to chromatographic column and discharge of remaining of gas flow to atmosphere. Delivery of carrier gas to evaporation chamber is effected in direction opposite to motion of evaporated sample to chromatographic column. Device proposed for introducing the sample into chromatograph has sample introducing line, evaporation chamber, chromatographic column, carrier gas supply and carrier gas discharge line which are connected with evaporation chamber. Carrier gas discharge line is connected with evaporation chamber in area of introduction of sample and carrier gas supply line is connected with opposite end of evaporation chamber.
EFFECT: enhanced accuracy of dosing the sample; improved quality of separation of components; enhanced reliability; simplified construction.
11 cl, 3 dwg
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Authors
Dates
2005-01-10—Published
2003-03-05—Filed