METHOD FOR EXTRACTION OF AMINONAPHTHOLSULFOACIDS AND AMINOPHENOLSULFOACIDS FROM AQUEOUS SOLUTIONS Russian patent published in 2005 - IPC

Abstract RU 2258698 C1

FIELD: organic chemistry, analytical chemistry, chemical technology.

SUBSTANCE: method for extraction of aminonaphtholsulfoacids and aminophenolsulfoacids involves extraction with organic solvent wherein sodium dodecyl sulfate an aqueous solution is added to aqueous solution up to its concentration 1.5 x 10-4 mol/dm3, hydrochloric acid is added up to the concentration 1.5-1.6 mol/dm3. As extractant method involves using 1,4-dioxane in the volume ratio of extractant to sample = 1:10 and extraction is carried out from saturated solution of ammonium sulfate. Invention provides enhancing degree of extraction of aminonaphtholmonosulfoacids and aminophenolmonosulfoacids from aqueous solutions wherein extraction degree of sulfoacids is 96.1-99.6% after a single extraction. Invention can be recommended for concentrating 1-amino-2-naphthol-4-sulfoacid and 2-aminophenol-4-sulfoacid from treated sewage waters in manufacturing azodyes.

EFFECT: improved method for extraction.

1 tbl, 11 ex

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RU 2 258 698 C1

Authors

Korenman Ja.I.

Gubin A.S.

Sukhanov P.T.

Dates

2005-08-20Published

2004-07-12Filed