FIELD: production of contact mass for reaction of powder silicon, alkyl halide and copper catalyst.
SUBSTANCE: proposed method includes forming mass by mixing silicon and copper source, heating to temperature of about 500°C and subjecting to heat treatment at temperature above 500°C where said heat treatment increases content of copper source Cu3Si in contact mass. Contact mass thus obtained is used as catalyst in production of alkylhalosilane including reaction between alkyl halide and silicon in presence of contact mass.
EFFECT: enhanced efficiency and selectivity.
9 cl, 4 tbl, 3 ex
Title | Year | Author | Number |
---|---|---|---|
METHOD OF ALKYLHALOIDSILANES SYNTHESIS | 0 |
|
SU1838316A3 |
METHOD FOR PREPARING METHYLCHLOROSILANES | 2003 |
|
RU2232764C1 |
METHOD FOR PROCESSING RESIDUES FROM SYNTHESIS OF ORGANOCHLOROSILANES AND/OR CHLOROSILANES WITH RECOVERY OF SILICON AND COPPER | 1995 |
|
RU2098501C1 |
METHOD OF PRODUCING ALKYLCHLORSILANES | 1991 |
|
RU2032688C1 |
METHOD OF SYNTHESIS OF TRIMETHYLCHLOROSILANE | 1995 |
|
RU2099343C1 |
METHOD FOR PRODUCTION OF METHYLCHLOROSILANES | 2001 |
|
RU2203900C2 |
PROCESS FOR PREPARING CONTACT COMPOSITION FOR SYNTHESIS OF CHLORO- OR ORGANOCHLOROSILANES | 0 |
|
SU1131877A1 |
METHOD FOR PRODUCTION OF METHYLCHLOROSILANES | 1994 |
|
RU2062779C1 |
METHOD OF METHYLCHLOROSILANES SYNTHESIS | 0 |
|
SU1733435A1 |
METHOD FOR PREPARING CONTACT MASS FOR DIRECT SYNTHESIS OF METHYLCHLOROSILANE IN BOILING LAYER | 2002 |
|
RU2220147C1 |
Authors
Dates
2005-11-27—Published
2001-02-20—Filed