FIELD: organic chemistry, chemical technology.
SUBSTANCE: invention proposes a method for preparing 3,4,5,6-tetrachloro-2-cyanopyridine by interaction of 2-cyanopyridine with chlorine in the presence of phosphorus chlorides as a catalyst taken in the amount 2-60 weight % of the initial loads of 2-cyanopyridine. The chlorination process is carried out in the melt at temperature 120-200°C and under pressure up to 0.6 MPa. Method provides simplifying the process by using the standard equipment, improving ecological indices and decreasing energy consumptions.
EFFECT: improved preparing method.
3 cl, 8 ex
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Authors
Dates
2006-03-20—Published
2004-06-04—Filed