METHOD OF PREPARING ACETYL CHLORIDE Russian patent published in 1999 - IPC

Abstract RU 2135457 C1

FIELD: manufacture of colorants, medicinals and other organic products. SUBSTANCE: acetyl chloride is prepared by reacting acetic acid with benzal chloride or stillage residues which result from benzyl chloride production and contain at least 38% of benzal chloride. Process is carried out at 90-125 C for 5.0-8.0 hours in the presence of 0.15-0.4 wt % of aluminium chloride, ferric chloride or zinc chloride. Final product is isolated by distillation. EFFECT: increased yield of acetyl chloride. 11 ex, 1 tbl

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RU 2 135 457 C1

Authors

Bogach E.V.

Kuznetsov A.A.

Mil'Gotin I.M.

Mokrushin M.V.

Poddubnyj I.S.

Roik F.I.

Sergeev A.A.

Telegin I.V.

Tkachuk L.N.

Mudryj F.V.

Dates

1999-08-27Published

1997-04-24Filed