FIELD: organic synthesis, more particularly method for production of new organoaluminum compounds.
SUBSTANCE: claimed method includes reaction of phenylallyl acetate with alkoxyaluminum dichloride in presence of magnesium metal and zirconacene dichloride as catalyst in argon atmosphere at room temperature in tetrahydrofuran for 8-12 hours.
EFFECT: simplified method, accessible reagents.
11 ex, 1 tbl
Title | Year | Author | Number |
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METHOD FOR PREPARING N, N, N, N-TETRAALKYL-4a,5,7a,8-TETRAHYDRO-1,3-DIPHENYLALUMINA[3,4-f]ISOALUMINAINDOL-2,6-(4H,7H)-DIAMINES | 2005 |
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RU2283316C1 |
METHOD FOR PREPARING 2,6-DIETHYL-5,7-DIPHENYL-1,2,3,3a,4,6,8,8a-OCTAHYDROALUMACYCLOPENTADIENO[3,4-f]-ISOALUMAINDOLE | 2004 |
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RU2280037C2 |
METHOD FOR PREPARING 1-CHLORO-3,4-DIALKYL-2,5-BIS-(TRIMETHYLSILYL)-ALUMINACYCLOPENTA-2,4-DIENES | 2005 |
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RU2295528C1 |
METHOD OF OBTAINING 1-CHLORO-3,4-DIALKYL-2,5-BIS[3-(1-ALKINYL)PHENYL]-1H-ALUMINOLS | 2007 |
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RU2348639C1 |
METHOD OF PRODUCING 10-ALKYL-12-ETHYL-12-ALUMINABICYCLO[7.3.0]DODEC-1( 2 )-ENES | 2008 |
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METHOD OF PRODUCING 9-ETHYL-11-ALKYL-9-ALUMINABICYCLO[6,3,0]UNDEC-1(8)-ENES | 2008 |
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METHOD OF PRODUCING 1-ETHYL-3-ALKYLALUMINIUM CYCLOPENTANES | 2009 |
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METHOD OF PRODUCING 2-ALKYL-1,4-BIS(DIETHYLALUMINIO)BUTANES | 2010 |
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RU2459828C2 |
METHOD FOR PREPARING 1-CHLORO-2,3,4,5-TETRAALKYLALUMINACYCLOPENTA-2,4-DIENES | 2005 |
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RU2283315C1 |
METHOD FOR COMBINED SYNTHESIS OF 1-ETHYL-2-ALKYLIDENEALUMINACYCLOPENTANES AND 1-ETHYL-2-METHYLENE-3-ALKYLALUMINACYCLOPENTANES | 2009 |
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RU2423370C2 |
Authors
Dates
2006-09-20—Published
2005-03-30—Filed