FIELD: organic chemistry, chemical technology.
SUBSTANCE: invention relates to synthesis of organic compounds. Acrylonitrile is hydrated in aqueous solution in the presence of a biocatalyst. Control for carrying out the reaction is carried out by measurements of parameters of the technological process in "on-line" regimen by infrared spectroscopy method with Fourier-transformation. The reaction is carried out in reactor fitted by circulation contour wherein part of the reaction mixture is pumped in closed cycle. Device comprises infrared spectrometer with Fourier-transformation providing carrying out measurements in "on-line" regimen rapidly and to retain activity of biocatalyst at the practically constant level in the reaction course and to produce larger amount of the more pure product.
EFFECT: improved method of synthesis.
16 cl, 1 dwg
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