FIELD: chemistry.
SUBSTANCE: method for the production of acrylamide from acrylonitrile and a device for carrying out the above method are provided. The device contains two or more connected in series A and B reactors, pipelines for supplying acrylonitrile, water and a catalyst in the upper stream of the reactor, a pipeline for releasing a part of the reaction liquid from the bottom of the reactor thread, a detection unit to determine the level of the reaction liquid in A reactor, and a control unit to regulate the volume of the reaction liquid. Moreover, the reactor A includes a circulating pipeline and a connecting hole with the reactor B located below the surfaces of the reaction liquids. The method includes regulating the volume of the reaction fluid in the reactor B through the control level of the reaction liquid in the reactor A, where the level of the reaction liquid in the reactor A is controlled by adjusting the volume of the reaction fluid that must be released and/or returned to the reactor A by circulation.
EFFECT: invention provides a duration of incubation of the reaction liquid in the reactor suitable for the production speed, reducing the amount of the catalyst used.
8 cl, 1 dwg, 1 tbl, 4 ex
Title | Year | Author | Number |
---|---|---|---|
METHOD FOR PRODUCING ACRYLAMIDE | 2013 |
|
RU2631650C2 |
CONTINUOUS METHOD FOR PRODUCTION OF AMIDE COMPOUND SUCH AS ACRYLAMIDE OR NICOTINEAMIDE | 2002 |
|
RU2279480C2 |
METHOD FOR PRODUCING A SOLUTION OF POLYACRYLAMIDE WITH INCREASED VISCOSITY | 2017 |
|
RU2751919C2 |
METHOD OF PRODUCING AQUEOUS SOLUTION OF ACRYLAMIDE UTILIZING BIOCATALYST | 2002 |
|
RU2317976C2 |
STABLE AQUEOUS ACRYLAMIDE SOLUTION | 2011 |
|
RU2573385C2 |
ACRYLAMIDE WATER SOLUTION, WHICH CONTAINS SACCHARIDE | 2003 |
|
RU2343161C2 |
METHOD FOR PREPARING ACRYLAMIDE AQUEOUS SOLUTION USING CATALYST | 2002 |
|
RU2289626C2 |
METHOD OF PRODUCING IMMOBILISED BIOCATALYST AND METHOD OF PRODUCING AQUEOUS AMIDE SOLUTIONS WITH USING THIS BIOCATALYST | 2007 |
|
RU2352635C2 |
AGENTS AND METHODS FOR PRODUCING AMIDE COMPOUNDS WITH LESS ACRYLIC ACID | 2015 |
|
RU2730624C2 |
IMPROVED BIOTECHNOLOGICAL PROCESS OF ACRYLAMIDE PRODUCING | 1998 |
|
RU2146291C1 |
Authors
Dates
2018-01-16—Published
2015-06-02—Filed