FIELD: organic chemistry, chemical technology.
SUBSTANCE: invention relates to a method for synthesis of linear unsaturated dimmers of α-methylstyrene that are used as modifying agents in manufacturing polymers. Method is carried out by the dimerization reaction in the presence of zeolite Y at the mole ratio SiO2/Al2O3 = 6.2-7.0 in NaH-form and ionic exchange degree 40-60%. The amount of catalyst is 1-5 wt.-%, the reaction temperature is 40-800C. Invention provides increasing working time of catalyst and improving indices of the process.
EFFECT: improved method of synthesis.
9 ex
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Authors
Dates
2007-12-27—Published
2006-03-27—Filed