ANILINE RECUPERATION METHOD Russian patent published in 2008 - IPC C07C209/82 C07C211/46 C07C209/36 

Abstract RU 2327683 C2

FIELD: chemistry.

SUBSTANCE: organic solvent is used as the extractant in the processes of obtaining or using aniline, with content of aniline in the solvent of 5% mass. Putting the extractant and the water solution into the extractor is done counter-flow. Recovery of the solvent is done through distillation of the obtained extract with obtaining of a residue, containing 10-40% mass of organic solvent. In particular, benzol can be used as the organic solvent, a by-product of the process of obtaining aniline through recovery of nitrobenzol using hydrogen. Recovery of the solvent is done in a distillation column for separating the by-product benzole from the fraction in the process of obtaining aniline.

EFFECT: lowering of heat consumption in the process of recuperating aniline from concentrated solutions by 11-13 times.

2 cl, 2 ex

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RU 2 327 683 C2

Authors

Agafonov Boris Aleksandrovich

Savel'Ev Aleksej Nikolaevich

Savel'Ev Nikolaj Ivanovich

Tikhonova Galina Georgievna

Khitrov Nikolaj Vjacheslavovich

Dates

2008-06-27Published

2006-05-04Filed