FIELD: chemistry.
SUBSTANCE: invention relates to the method of obtaining the derivatives 3-aroilanra-(1,9-cd)isoxazole-6-one of the general formula where X - hydrogen, halogen or the lowest alkyl, which are used as intermediate products in synthesis of derivatives 7,8-phthalylclaridone used as dyes for various polymeric materials and polyester fibres. The essence of the method lies in boiling 1(triazene-N-sulfonate)-2-aroihtranquonine in spirit solution of alkali with the subsequent neutralisation by acetic acid.
EFFECT: simpler technology and safer process.
1 cl, 2 tbl, 3 ex
Title | Year | Author | Number |
---|---|---|---|
METHOD OF 7,8-PHTALOYLACRIDONE DERIVATIVES PRODUCTION | 2007 |
|
RU2332407C1 |
METHOD OF OBTAINING DERIVED 3-AROILANTRA-(1,9-cd)ISOXAZOLE-6-ONE | 2007 |
|
RU2330028C1 |
METHOD OF 7,8-PHTALOYLACRIDONE DERIVATIVES PRODUCTION | 2007 |
|
RU2332406C1 |
METHOD FOR PREPARING DERIVATIVES OF 3-PHENYLSULFONYLANTHRA-[1,9-cd]-ISOXAZOLE-6-ONE | 2005 |
|
RU2276144C1 |
METHOD FOR PREPARING DERIVATIVES OF 3-PHENYLSULFONYLANTHRA-[1,9-cd]-ISOXAZOLE-6-ONE | 2005 |
|
RU2276143C1 |
METHOD FOR PRODUCTION OF DERIVATIVES OF 3-PHENYLTHIOANTHRA/1,9-CD/ISOXAZOLE-6-ON | 1994 |
|
RU2074183C1 |
METHOD FOR PRODUCTION OF DERIVATIVES OF 3-PHENYLOXY-5-HYDROXYANTHRA-[1,9-CD]ISOXAZOL-6-ON | 1993 |
|
RU2065438C1 |
METHOD FOR PREPARING DERIVATIVES OF 5,6-PHTHALYLPHENOTHIAZINE-S,S-DIOXIDE | 2005 |
|
RU2276145C1 |
METHOD FOR PREPARING DERIVATIVES OF 5,6-PHTHALYLPHENOTHIAZINE-S,S-DIOXIDE | 2005 |
|
RU2277088C1 |
METHOD FOR PRODUCTION OF DERIVATIVES OF 5,6-PHTHALYL PHENOTHIAZINE | 1994 |
|
RU2072356C1 |
Authors
Dates
2008-07-27—Published
2007-05-21—Filed